ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

Base Information

Chemical Name:ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate
CAS No.:1615657-82-3
Molecular Formula:C₂₁H₂₁ClO₄
Molecular Weight:372.848
Hs Code.:

Synonyms:ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

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Chemical Property of ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

Chemical Property:

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Technology Process of ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

There total 1 articles about ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 127776-17-4
1-(bromomethyl)-4-(4-chlorophenoxy)benzene

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 1615657-82-3
ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃;

Reference yield:

: 1615657-82-3
ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

: 1615657-85-6
ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-3,3-dimethyl-2-oxocyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -78 °C

2.2: -78 - 20 °C

With lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran;

Reference yield:

: 1615657-82-3
ethyl 1-[[4-(4-chlorophenoxy)phenyl]methyl]-2-oxocyclopentanecarboxylate

: 1615657-86-7
5-[[4-(4-chlorophenoxy)phenyl]methyl]-2,2-dimethylcyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -78 °C

2.2: -78 - 20 °C

3.1: sodium hydroxide; water / isopropyl alcohol / Reflux

With water; sodium hydroxide; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; isopropyl alcohol;