Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

Base Information

Chemical Name:Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester
CAS No.:210298-03-6
Molecular Formula:C₂₂H₂₇NO₅Si
Molecular Weight:413.546
Hs Code.:

Synonyms:Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

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Chemical Property of Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

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Technology Process of Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

There total 7 articles about Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 75611-67-5
Pyran-2-one-6-carbonyl chloride

: 210298-01-4
Isobutyric acid [(benzylamino-methyl)-methyl-vinyl-silanyl]-methyl ester

: 210298-03-6
Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(98)00698-4

Reference yield:

: 100-46-9
benzylamine

: 210298-03-6
Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 100 °C

2: 93 percent / NEt₃ / CH₂Cl₂ / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(98)00698-4

Reference yield:

: 210297-90-8
(Hydroxymethyl-methyl-vinyl-silanyl)-methanol

: 210298-03-6
Isobutyric acid ({[benzyl-(6-oxo-6H-pyran-2-carbonyl)-amino]-methyl}-methyl-vinyl-silanyl)-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / Lipase from Candida rugosa / 24 h / 20 °C

2: 98 percent / CBr₄, PPh₃ / CH₂Cl₂ / Ambient temperature

3: 67 percent / 100 °C

4: 93 percent / NEt₃ / CH₂Cl₂ / 0 °C

With carbon tetrabromide; lipase from Candida rugosa; triethylamine; triphenylphosphine; In dichloromethane;
DOI:10.1016/S0040-4039(98)00698-4