C₁₃H₁₀ClFS

Base Information

• Chemical Name: C₁₃H₁₀ClFS
• CAS No.: 887079-34-7
• Molecular Formula: C₁₃H₁₀ClFS
• Molecular Weight: 252.74
• Mol file: 887079-34-7.mol

Synonyms:C₁₃H₁₀ClFS

Chemical Property of C₁₃H₁₀ClFS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₀ClFS

There total 2 articles about C₁₃H₁₀ClFS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-Fluorotoluene (95-52-3) + p-Chlorothiophenol (106-54-7) → C13H10ClFS (887079-34-7)

Guidance literature:

With tert.-butylhydroperoxide; oxygen; palladium diacetate; In water; at 115 ℃; for 24h; under 760.051 Torr;

DOI:10.1039/c4ra09450f

Reference yield:

o-fluorobenzyl bromide (446-48-0) + p-Chlorothiophenol (106-54-7) → C13H10ClFS (887079-34-7)

Guidance literature:

With triethylamine;

DOI:10.1016/j.bmcl.2004.12.017

Reference yield:

C13H10ClFS (887079-34-7) → C18H18ClFO2S

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloroperoxybenzoic acid

2: NaH / dimethylformamide / 8 h / 20 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2004.12.017

upstream raw materials:

o-fluorobenzyl bromide

p-Chlorothiophenol

2-Fluorotoluene

Downstream raw materials:

C₁₃H₁₀ClFO₂S