10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside
CAS No.:574737-37-4
Molecular Formula:C₇₁H₈₃N₃O₁₁
Molecular Weight:1154.45
Hs Code.:

Synonyms:10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

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Chemical Property of 10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

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Technology Process of 10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

There total 9 articles about 10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 574737-36-3
10-azidodecyl 2,3,6-tri-O-benzyl-β-D-galactopyranoside

: 4291-68-3,25320-59-6,41110-63-8,67068-83-1,67773-44-8,69237-96-3,92470-93-4,93601-69-5,113829-62-2
(2R,3S,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-chloro-tetrahydro-pyran

: 10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

: 574737-37-4
10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: 10-azidodecyl 2,3,6-tri-O-benzyl-β-D-galactopyranoside; (2R,3S,4S,5R,6R)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-chloro-tetrahydro-pyran; With 4 A molecular sieve; In diethyl ether; for 1h;

With silver perchlorate; In diethyl ether; at 25 ℃; for 22h;
DOI:10.1016/j.tet.2005.03.102

Reference yield:

: 860036-11-9
10-azidodecyl β-D-galactopyranoside

: 574737-37-4
10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: 392 mg / camphorsulfonic acid / acetone / 2.5 h / 25 °C

2.1: 100 percent / NaH / dimethylformamide / 2 h / 25 °C

3.1: 84 percent / camphorsulfonic acid / methanol / 2 h / 25 °C

4.1: Bu₂SnO / toluene / 6 h / Heating

4.2: 93 percent / Bu₄NBr / toluene / 3 h / 25 °C

5.1: molecular sieves 4 Angstroem / diethyl ether / 1 h

5.2: 67 percent / AgClO₄ / diethyl ether / 22 h / 25 °C

With 4 A molecular sieve; camphor-10-sulfonic acid; sodium hydride; di(n-butyl)tin oxide; In methanol; diethyl ether; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2005.03.102

Reference yield:

: 574737-33-0
10-azidodecyl 3,4-O-isopropylidene-β-D-galactopyranoside

: 574737-37-4
10-azadodecyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / NaH / dimethylformamide / 2 h / 25 °C

2.1: 84 percent / camphorsulfonic acid / methanol / 2 h / 25 °C

3.1: Bu₂SnO / toluene / 6 h / Heating

3.2: 93 percent / Bu₄NBr / toluene / 3 h / 25 °C

4.1: molecular sieves 4 Angstroem / diethyl ether / 1 h

4.2: 67 percent / AgClO₄ / diethyl ether / 22 h / 25 °C

With 4 A molecular sieve; camphor-10-sulfonic acid; sodium hydride; di(n-butyl)tin oxide; In methanol; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2005.03.102