2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Base Information

Chemical Name:2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol
CAS No.:1415680-12-4
Molecular Formula:C₂₃H₂₈O₁₃
Molecular Weight:512.468
Hs Code.:

Synonyms:2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Suppliers and Price of 2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

There total 4 articles about 2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1415680-10-2
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-5-acetyloxybenzaldehyde

: 1415680-12-4
2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Guidance literature:: With sodium tetrahydroborate; cetyltrimethylammonim bromide; In chloroform; water; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2012.10.006

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1415680-12-4
2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 2 h / 110 °C

2: trifluoroacetic acid / 1 h / 80 °C

3: silver(l) oxide / quinoline / 1 h / 20 °C

4: sodium tetrahydroborate; cetyltrimethylammonim bromide / water; chloroform / 2 h / 20 °C

With sodium tetrahydroborate; cetyltrimethylammonim bromide; acetic acid; trifluoroacetic acid; silver(l) oxide; In quinoline; chloroform; water;
DOI:10.1016/j.carres.2012.10.006

Reference yield:

: 64418-88-8
2-hydroxy-5-acetyloxybenzaldehyde

: 1415680-12-4
2-(2,3,4,6-tetra-О-acetyl-β-D-glucopyranozyloxy)-5-acetyloxybenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: silver(l) oxide / quinoline / 1 h / 20 °C

2: sodium tetrahydroborate; cetyltrimethylammonim bromide / water; chloroform / 2 h / 20 °C

With sodium tetrahydroborate; cetyltrimethylammonim bromide; silver(l) oxide; In quinoline; chloroform; water;
DOI:10.1016/j.carres.2012.10.006