N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide

Base Information

• Chemical Name: N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide
• CAS No.: 1016571-73-5
• Molecular Formula: C₅₈H₆₀N₄O₆
• Molecular Weight: 909.138

Synonyms:N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide

Chemical Property of N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide

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Technology Process of N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide

There total 1 articles about N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-(2,2-diphenylethyl)-2-oxa-7-azapyrene-1,3,6,8-tetraone (1016571-72-4) + N1-(12-aminododecyl)-N4-(2,2-diphenylethyl)succinamide (573986-14-8) → N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide (1016571-73-5)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 4h;

DOI:10.1021/ja077223a

Reference yield: 35.0%

pyridine-3,5-dicarbonyl dichloride (15074-61-0) + N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide (1016571-73-5) + p-xylylidenediamine (539-48-0) → [2]-(1,7,14,20-tetraaza-2,6,15,19-tetraoxo-9,12,22,25-dibenzo-3,5,16,18-di[5-pyridyl]cyclohexacosane)-[N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)-naphthalene-1,4,5,8-tetracarboxylic diimide]-rotaxane (1016571-75-7)

Guidance literature:

With triethylamine; In chloroform; for 20h;

DOI:10.1021/ja077223a

Reference yield: 28.0%

N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)naphthalene-1,4,5,8-tetracarboxylic diimide (1016571-73-5) + p-xylylidenediamine (539-48-0) + benzene-1,3-dicarbonyl dichloride (99-63-8) → [2]-(1,7,14,20-tetraaza-2,6,15,19-tetraoxo-3,5,9,12,16,18,22,25-tetrabenzocyclohexacosane)-[N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)-naphthalene-1,4,5,8-tetracarboxylic diimide]-rotaxane (1016571-74-6)

Guidance literature:

With triethylamine; In chloroform; for 6h;

DOI:10.1021/ja077223a

upstream raw materials:

7-(2,2-diphenylethyl)-2-oxa-7-azapyrene-1,3,6,8-tetraone

N¹-(12-aminododecyl)-N⁴-(2,2-diphenylethyl)succinamide

Downstream raw materials:

[2]-(1,7,14,20-tetraaza-2,6,15,19-tetraoxo-9,12,22,25-dibenzo-3,5,16,18-di[5-pyridyl]cyclohexacosane)-[N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)-naphthalene-1,4,5,8-tetracarboxylic diimide]-rotaxane

[2]-(1,7,14,20-tetraaza-2,6,15,19-tetraoxo-3,5,9,12,16,18,22,25-tetrabenzocyclohexacosane)-[N-(2,2-diphenylethyl)-N'-(12-{[4-(2,2-diphenylethylamino)-4-oxobutanoyl]amino}dodecyl)-naphthalene-1,4,5,8-tetracarboxylic diimide]-rotaxane

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