(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

Base Information

Chemical Name:(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride
CAS No.:1233561-12-0
Molecular Formula:C₁₃H₁₉NO*ClH
Molecular Weight:241.761
Hs Code.:

Synonyms:(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

Chemical Property:

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Technology Process of (1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

There total 3 articles about (1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1233561-11-9
tert-butyl {(1R,3S)-3-[(benzyloxy)methyl]cyclopentyl}carbamate

: 1233561-12-0
(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 261165-05-3
(1S,3R)-3-(tert-butoxycarbonylamino)cyclopentanecarboxylic acid

: 1233561-12-0
(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 0.75 h / -20 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; mineral oil / 0.75 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 12 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; mineral oil;

Reference yield:

: 347185-68-6,167081-31-4,497159-95-2
tert-butyl ((1R,3S)-3-(hydroxymethyl)cyclopentyl)carbamate

: 1233561-12-0
(1R,3S)-3-[(benzyloxy)methyl]cyclopentanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; mineral oil / 0.75 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 12 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; mineral oil;