N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

Base Information

Chemical Name:N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine
CAS No.:748874-70-6
Molecular Formula:C₂₂H₂₂BrNO₄
Molecular Weight:444.325
Hs Code.:

Synonyms:N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

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Technology Process of N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

There total 4 articles about N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 214123-07-6
6-bromo-3-hydroxy-2-methoxybenzaldehyde

: 748874-70-6
N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / K₂CO₃ / dimethylformamide / 2 h / 100 °C

2: ethanol / 2 h / Heating

3: 569 mg / NaBH₄ / ethanol / 1 h / Heating

With sodium tetrahydroborate; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-822371

Reference yield:

: [1-(6-Bromo-3-isopropoxy-2-methoxy-phenyl)-meth-(Z)-ylidene]-naphtho[2,3-d][1,3]dioxol-5-yl-amine

: 748874-70-6
N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 1h; Heating;
DOI:10.1055/s-2004-822371

Reference yield:

: 748874-59-1
6-bromo-3-isopropoxy-2-methoxybenzaldehyde

: 748874-70-6
N-(6-bromo-3-isopropoxy-2-methoxybenzyl)-6,7-methylenedioxy-1-naphthylamine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 2 h / Heating

2: 569 mg / NaBH₄ / ethanol / 1 h / Heating

With sodium tetrahydroborate; In ethanol;
DOI:10.1055/s-2004-822371