Technology Process of C8H5BrF2O2
There total 5 articles about C8H5BrF2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
methanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hydroxide; water / 3 h / 20 °C
2: N,N-dimethyl-formamide / 20 °C
3: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 1.5 h / Cooling with ice
4: difluoro-4-morpholinylsulfonium tetrafluoroborate; triethylamine tris(hydrogen fluoride) / dichloromethane / 20 °C / Cooling with ice
5: lithium hydroxide; water / methanol / 20 °C
With
water; sulfur trioxide pyridine complex; difluoro-4-morpholinylsulfonium tetrafluoroborate; triethylamine tris(hydrogen fluoride); triethylamine; lithium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethyl-formamide / 20 °C
2: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 1.5 h / Cooling with ice
3: difluoro-4-morpholinylsulfonium tetrafluoroborate; triethylamine tris(hydrogen fluoride) / dichloromethane / 20 °C / Cooling with ice
4: lithium hydroxide; water / methanol / 20 °C
With
water; sulfur trioxide pyridine complex; difluoro-4-morpholinylsulfonium tetrafluoroborate; triethylamine tris(hydrogen fluoride); triethylamine; lithium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;