Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

Base Information

Chemical Name:Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide
CAS No.:82098-78-0
Molecular Formula:C₂₅H₂₅N₃O₄S
Molecular Weight:463.557
Hs Code.:

Synonyms:Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

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Chemical Property of Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

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Technology Process of Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

There total 6 articles about Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 110-91-8,99108-56-2
morpholine

: 82098-62-2
4-(4-Cyano-phenyl)-2-(naphthalene-2-sulfonylamino)-butyryl chloride

: 82098-78-0
Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

Guidance literature:: In benzene; Ambient temperature;

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 82098-78-0
Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / H₂ / Raney-nickel / methanol / Ambient temperature

2: 1.) NaNO₂/conc. HCl; 2.) CuCN/NaCN / 1.) H₂O, 0-5 deg C; 2.) benzene, 0-5 deg C, 30 min; room temp., 4 h

3: 63 percent / PBr₃ / CHCl₃ / 1.5 h / Heating

4: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

6: 97.5 percent / benzene / Ambient temperature

With hydrogenchloride; sodium cyanide; hydrogen; sodium; phosphorus tribromide; potassium iodide; sodium nitrite; nickel; In methanol; chloroform; benzene;

Reference yield:

: 72054-56-9
4-(2-bromoethyl)benzonitrile

: 82098-78-0
Naphthalene-2-sulfonic acid [3-(4-cyano-phenyl)-1-(morpholine-4-carbonyl)-propyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

3: 97.5 percent / benzene / Ambient temperature

With sodium; potassium iodide; In benzene;