7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

Base Information

Chemical Name:7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione
CAS No.:1169662-62-7
Molecular Formula:C₂₀H₂₂F₂N₄S
Molecular Weight:388.484
Hs Code.:

Synonyms:7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

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Chemical Property of 7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

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Technology Process of 7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

There total 3 articles about 7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1088437-54-0
C₁₉H₁₉F₂NO

: 79-19-6
thiosemicarbazide

: 1169662-62-7
7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; for 0.05h; Microwave irradiation; Neat (no solvent);
DOI:10.1007/s10593-011-0720-5

Reference yield: 60.0%

: 1169662-52-5
C₂₀H₂₂F₂N₄S

: 1169662-62-7
7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 0.75h;
DOI:10.1007/s10593-011-0720-5

Reference yield:

: 1088437-54-0
C₁₉H₁₉F₂NO

: 1169662-62-7
7,9-bis(4-fluorophenyl)-6,6-dimethyl-1,2,4,8-tetraazaspiro[4.5]decane-3-thione

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 2 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / 0 - 5 °C

With 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1007/s10593-011-0720-5