C₁₄H₁₇BrO₃

Base Information

Chemical Name:C₁₄H₁₇BrO₃
CAS No.:1269411-33-7
Molecular Formula:C₁₄H₁₇BrO₃
Molecular Weight:313.191
Hs Code.:

C<sub>14</sub>H<sub>17</sub>BrO<sub>3</sub>

Synonyms:C₁₄H₁₇BrO₃

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Chemical Property of C₁₄H₁₇BrO₃

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Technology Process of C₁₄H₁₇BrO₃

There total 4 articles about C₁₄H₁₇BrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1269411-32-6
C₁₄H₁₆BrNO₂

: 1269411-33-7
C₁₄H₁₇BrO₃

Guidance literature:: With formic acid; water; at 100 ℃; for 1h;
DOI:10.1016/j.bmcl.2010.12.034

Reference yield:

: 1086429-87-9
2-bromo-3-(bromomethyl)benzonitrile

: 1269411-33-7
C₁₄H₁₇BrO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.92 h / -20 °C / Inert atmosphere

1.2: 0.75 h / -20 °C

2.1: formic acid; water / 1 h / 100 °C

With n-butyllithium; formic acid; water; diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2010.12.034

Reference yield:

: C₁₂H₁₃BrO₄

: 1269411-33-7
C₁₄H₁₇BrO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonium hydroxide / 0.03 h / 0 °C

2.1: 1,3,5-trichloro-2,4,6-triazine / N,N-dimethyl-formamide / 0 - 20 °C

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 16 h / Reflux; Inert atmosphere

4.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.92 h / -20 °C / Inert atmosphere

4.2: 0.75 h / -20 °C

5.1: formic acid; water / 1 h / 100 °C

With ammonium hydroxide; N-Bromosuccinimide; n-butyllithium; formic acid; 1,3,5-trichloro-2,4,6-triazine; water; diisopropylamine; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.034