Technology Process of C59H69N3O22
There total 1 articles about C59H69N3O22 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
acetone;
at -5 ℃;
for 1.5h;
DOI:10.1246/cl.1984.2097
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridine
2: 1.) BF3-Et2O; 2.) Jones reagent / 1.) THF, 2 deg C, 40 min; 2.) r.t., 4 h
3: benzene; pyridine / 1 h / Heating
4: 62 percent / NaOMe / methanol; nitromethane / 14 h / Ambient temperature
5: 1.) p-TsOH*H2O; 2.) pyridine; 3.) d-10-camphorsulfonic acid / 1.) DMF, 45 deg C, 50 min; 2.) r.t., 8 h; 3.) DMF, r.t., 10 min
7: 59 percent / 80percent aq. NH2NH2*H2O / 66 h / 100 °C / sealed tube
With
pyridine; jones reagent; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; hydrazine hydrate;
In
pyridine; methanol; nitromethane; benzene;
DOI:10.1246/cl.1984.2097
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine
2: 1.) BF3-Et2O; 2.) Jones reagent / 1.) THF, 2 deg C, 40 min; 2.) r.t., 4 h
3: benzene; pyridine / 1 h / Heating
4: 62 percent / NaOMe / methanol; nitromethane / 14 h / Ambient temperature
5: 1.) p-TsOH*H2O; 2.) pyridine; 3.) d-10-camphorsulfonic acid / 1.) DMF, 45 deg C, 50 min; 2.) r.t., 8 h; 3.) DMF, r.t., 10 min
With
pyridine; jones reagent; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid;
In
pyridine; methanol; nitromethane; benzene;
DOI:10.1246/cl.1984.2097
