(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

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Chemical Name:(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole
CAS No.:185609-04-5
Molecular Formula:C₂₄H₃₅NO₆
Molecular Weight:433.545
Hs Code.:

Synonyms:(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

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Chemical Property of (3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

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Technology Process of (3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

There total 1 articles about (3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-46-9
benzylamine

: Methanesulfonic acid (S)-((4S,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-methyl ester

: 185609-04-5
(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

Guidance literature:: at 110 ℃; for 48h;
DOI:10.1016/0040-4039(96)01956-9

Reference yield: 68.0%

: 185609-04-5
(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

: 185609-05-6
(R)-1-[(4R,5R)-5-((3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-ethane-1,2-diol

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1016/0040-4039(96)01956-9

Reference yield:

: 185609-04-5
(3aR,4R,6aS)-5-Benzyl-2,2-dimethyl-4-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole

: 185609-06-7
Methanesulfonic acid (R)-2-[(4R,5R)-5-((3aR,4R,6aS)-5-benzyl-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyrrol-4-yl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-2-hydroxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / p-toluenesulfonic acid / methanol

2: 91 percent / 4-dimethylamino-pyridine / pyridine

With dmap; toluene-4-sulfonic acid; In pyridine; methanol;
DOI:10.1016/0040-4039(96)01956-9