C₁₂H₁₅⁽²⁾HO₇

Base Information

Chemical Name:C₁₂H₁₅⁽²⁾HO₇
CAS No.:91758-40-6
Molecular Formula:C₁₂H₁₆O₇
Molecular Weight:273.247
Hs Code.:

C<sub>12</sub>H<sub>15</sub><sup>(2)</sup>HO<sub>7</sub>

Synonyms:C₁₂H₁₅⁽²⁾HO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₅⁽²⁾HO₇

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Technology Process of C₁₂H₁₅⁽²⁾HO₇

There total 10 articles about C₁₂H₁₅⁽²⁾HO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 91758-37-1
C₁₈H₂₉⁽²⁾HO₇Si

: 91758-40-6
C₁₂H₁₅⁽²⁾HO₇

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 5 ℃; for 0.5h;
DOI:10.1016/S0040-4039(00)85910-9

Reference yield:

: 88400-31-1
(3aR,7R,7aS)-7-Hydroxy-2-methoxy-2-methyl-3a,6,7,7a-tetrahydro-benzo[1,3]dioxole-5-carboxylic acid methyl ester

: 91758-40-6
C₁₂H₁₅⁽²⁾HO₇

Guidance literature:: Multi-step reaction with 8 steps

1: imidazole / dimethylformamide / 1 h / 45 °C / under nitrogen gas

2: water / conc. HCl / methanol / 1 h / Ambient temperature

3: pyridinium dichromate / dimethylformamide / 1 h / 45 °C / under nitrogen gas

4: NaBD₄ / ethanol / 0.25 h / 5 °C

5: NEt₃ / CH₂Cl₂ / 0.25 h / 5 °C / under nitrogen gas

6: potassium acetate / 1.5 h / 70 °C

7: 1.) water / 1.) conc. HCl / 1.) methanol, room temp., 1h; 2.) re-acetylation

8: 83 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 5 °C

With 1H-imidazole; dipyridinium dichromate; sodium borodeuteride; tetrabutyl ammonium fluoride; water; potassium acetate; triethylamine; hydrogenchloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85910-9

Reference yield:

: 88400-34-4
(4S,5R)-4-Acetoxy-5-(tert-butyl-dimethyl-silanyloxy)-3-oxo-cyclohex-1-enecarboxylic acid methyl ester

: 91758-40-6
C₁₂H₁₅⁽²⁾HO₇

Guidance literature:: Multi-step reaction with 5 steps

1: NaBD₄ / ethanol / 0.25 h / 5 °C

2: NEt₃ / CH₂Cl₂ / 0.25 h / 5 °C / under nitrogen gas

3: potassium acetate / 1.5 h / 70 °C

4: 1.) water / 1.) conc. HCl / 1.) methanol, room temp., 1h; 2.) re-acetylation

5: 83 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 5 °C

With sodium borodeuteride; tetrabutyl ammonium fluoride; water; potassium acetate; triethylamine; hydrogenchloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/S0040-4039(00)85910-9