N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

Base Information

Chemical Name:N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt
CAS No.:919528-60-2
Molecular Formula:C₂HF₃O₂*C₃₅H₄₃N₅O₆
Molecular Weight:743.78
Hs Code.:

N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

Synonyms:N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

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Chemical Property of N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

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Technology Process of N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

There total 1 articles about N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 919527-94-9
(2R)-2-[(tert-butoxy)carbonylamino]-N-[(fluoren-9-ylmethoxy)carbonylamino]-4-methylpentanamide

: 848084-15-1
tert-butyl (S)-(4-methyl-1-((4-((((4-nitrophenoxy)carbonyl)oxy)methyl)phenyl)amino)-1-oxopentan-2-yl)carbamate

: 76-05-1
trifluoroacetic acid

: 919528-60-2
N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

Guidance literature:: (2R)-2-[(tert-butoxy)carbonylamino]-N-[(fluoren-9-ylmethoxy)carbonylamino]-4-methylpentanamide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

tert-butyl (S)-(4-methyl-1-((4-((((4-nitrophenoxy)carbonyl)oxy)methyl)phenyl)amino)-1-oxopentan-2-yl)carbamate; With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.333333h;

Reference yield: 38.0%

: Ac-PL-NLys(Boc)-Hphe-OH

: 919528-60-2
N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt

: 76-05-1
trifluoroacetic acid

: N-[(N-{1-[N-(1-{N-[4-({N-[(1R)-1-(N-aminocarbamoyl)-3-methylbutyl]carbamoyloxy}methyl)phenyl]carbamoyl}(1S)-3-methylbutyl)-carbamoyl](1S)-3-phenylpropyl}carbamoyl)methyl](2S)-2-[((2S)-1-acetylpyrrolidin-2-yl)carbonylamino]-N-{4-[(tert-butoxy)carbonylamino]butyl}-4-methylpentanamide trifluoroacetic acid salt

Guidance literature:: Ac-PL-NLys(Boc)-Hphe-OH; N-(4-{[N-((1R)-1-{N-[(fluoren-9-ylmethoxy)-carbonylamino]carbamoyl}-3-methylbutyl)carbamoyloxy]methyl}phenyl)(2S)-2-amino-4-methylpentanamide trifluoroacetic acid salt; With 2,3,4-lutidine; 1-hydroxy-7-aza-benzotriazole; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

With 2,2',2''-triaminotriethylamine; In N,N-dimethyl-formamide; for 0.333333h;

trifluoroacetic acid; In acetonitrile;