4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide

Base Information Edit

Chemical Name:4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide
CAS No.:1330740-28-7
Molecular Formula:C₃₁H₃₂N₂O₅
Molecular Weight:512.605
Hs Code.:
Mol file:1330740-28-7.mol

Synonyms:4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide

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Chemical Property of 4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide Edit

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Technology Process of 4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide

There total 2 articles about 4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1330740-26-5
5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethyl-4-ethynylisoxazole-3-carboxamide

: 1330740-28-7
4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide

Guidance literature:: 5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethyl-4-ethynylisoxazole-3-carboxamide; With formic acid; at 95 ℃; for 1h;

With sodium hydrogencarbonate; pH=8;

Reference yield:

: 747414-22-8
5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-4-iodoisoxazole-3-carboxylic acid ethylamide

: 1330740-28-7
4-acetyl-5-(2,4-bis(benzyloxy)-5-isopropylphenyl)-N-ethylisoxazole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 0.17 h / 112 °C

1.2: 2 h / Reflux

2.1: formic acid / 1 h / 95 °C

2.2: pH 8

With formic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;