C₃₀H₂₈O₉

Base Information

• Chemical Name: C₃₀H₂₈O₉
• CAS No.: 1418141-20-4
• Molecular Formula: C₃₀H₂₈O₉
• Molecular Weight: 532.547
• Mol file: 1418141-20-4.mol

Synonyms:C₃₀H₂₈O₉

Chemical Property of C₃₀H₂₈O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₈O₉

There total 8 articles about C₃₀H₂₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C29H28O8 (1448861-31-1) + acetic anhydride (108-24-7) + acetic acid (64-19-7,77671-22-8) → C30H28O9 (1418141-20-4)

Guidance literature:

With sulfuric acid; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

C10H16O5 (1417563-63-3) → C30H28O9 (1418141-20-4)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrahydrofuran; diethyl ether / 6 h / -78 - 10 °C

2: pyridine; dmap / dichloromethane / 15 h / 20 °C

3: trifluoroacetic acid; water / 1 h

4: dmap; triethylamine / acetonitrile / 60 h

5: sulfuric acid / dichloromethane / 2 h / 0 °C

With pyridine; dmap; sulfuric acid; water; triethylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

C18H24O6 (1417563-65-5) → C30H28O9 (1418141-20-4)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid; water / 1 h

2: dmap; triethylamine / acetonitrile / 60 h

3: sulfuric acid / dichloromethane / 2 h / 0 °C

With dmap; sulfuric acid; water; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;

upstream raw materials:

C₁₀H₁₆O₅

C₁₁H₂₀O₅

C₁₈H₂₄O₆

C₁₅H₂₀O₆

Downstream raw materials:

C₃₉H₃₃N₃O₉

C₃₂H₂₈N₂O₉