2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

Base Information

Chemical Name:2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine
CAS No.:1609583-53-0
Molecular Formula:C₂₄H₁₈N₂O₂S₂
Molecular Weight:430.551
Hs Code.:

Synonyms:2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

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Chemical Property of 2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

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Technology Process of 2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

There total 3 articles about 2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 529-36-2
1-Naphthalenethiol

: 1222-57-7
zolimidine

: 1609583-53-0
2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

Guidance literature:: 1-Naphthalenethiol; With N-chloro-succinimide; In dichloromethane; for 0.5h;

zolimidine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmcl.2021.128307

Reference yield:

: 504-29-0
2-aminopyridine

: 1609583-53-0
2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate; copper(l) iodide / N,N-dimethyl-formamide / 24 h / 60 °C

2.1: N-chloro-succinimide / dichloromethane / 0.5 h

2.2: 0.5 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; copper(l) iodide; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2021.128307

Reference yield:

: 10297-73-1
4-(methanesulfonyl)acetophenone

: 1609583-53-0
2-(4-(methylsulfonyl)phenyl)-3-(naphthalen-1-ylthio)imidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate; copper(l) iodide / N,N-dimethyl-formamide / 24 h / 60 °C

2.1: N-chloro-succinimide / dichloromethane / 0.5 h

2.2: 0.5 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; copper(l) iodide; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2021.128307