bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)

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Chemical Name:bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)
CAS No.:219802-71-8
Molecular Formula:C₂₄H₂₀OS₂Ti
Molecular Weight:436.434
Hs Code.:

Synonyms:bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)

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Chemical Property of bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)

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Technology Process of bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)

There total 1 articles about bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 219802-62-7
C₆H₃(SH)2C(O)N(C₂H₅)2

: 219802-68-3
C₆H₃(SH)2C(O)CH₂C₆H₅

: 219802-70-7
bis(η(5)-cyclopentadienyl)(N,N-diethylbenzamide-2,3-dithiolato)titanium(IV)

: 219802-71-8
bis(η(5)-cyclopentadienyl)[(2-phenyl-1-oxoethyl)benzene-2,3-dithiolato]titanium(IV)

Guidance literature:: With Et₃N; In tetrahydrofuran; Ar-atmosphere; mixing Ti-complex with diethylamino-ligand (contg. deaminated ligand as impurity), Et3N addn., stirring for 2 h; solvent removal, chromy. (SiO2, CH2Cl2/Et2O=1:1); elem. anal.;
DOI:10.1021/ic9706616