1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

Base Information

Chemical Name:1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl
CAS No.:1286784-13-1
Molecular Formula:C₄₂H₈₈Si₆
Molecular Weight:761.674
Hs Code.:

Synonyms:1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

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Chemical Property of 1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

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Technology Process of 1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

There total 3 articles about 1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1286784-12-0
1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-1-iodo-2-methyldisilanyl]benzene

: 1286784-13-1
1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

Guidance literature:: With KC₈; In tetrahydrofuran; at -78 - 20 ℃; for 7h;
DOI:10.1021/ja2014746

Reference yield:

: 1,3-[K(t-Bu₂MeSi)2Si]2C₆H₄

: 1286784-13-1
1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

Guidance literature:: Multi-step reaction with 2 steps

1: iodine / tetrahydrofuran

2: KC₈ / tetrahydrofuran / 7 h / -78 - 20 °C

With iodine; In tetrahydrofuran;
DOI:10.1021/ja2014746

Reference yield:

: 1286784-16-4
1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene

: 1286784-13-1
1,3-bis[2,2-di-tert-butyl-1-(di-tert-butylmethylsilyl)-2-methyldisilanyl]benzene-1',1''-diyl

Guidance literature:: Multi-step reaction with 3 steps

1: potassium / tetrahydrofuran / 26 h / 20 °C

2: iodine / tetrahydrofuran

3: KC₈ / tetrahydrofuran / 7 h / -78 - 20 °C

With iodine; potassium; In tetrahydrofuran;
DOI:10.1021/ja2014746