(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

Base Information

Chemical Name:(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene
CAS No.:669692-96-0
Molecular Formula:C₃₉H₂₇N₃O₁₂
Molecular Weight:729.656
Hs Code.:

Synonyms:(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

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Chemical Property of (+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

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Technology Process of (+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

There total 3 articles about (+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 669692-90-4
(+/-)-2,7,12-tris(4-nitrophenoxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[adg]cyclononene

: 669692-96-0
(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

Guidance literature:: With boron tribromide; In toluene; at 90 ℃; for 12h;
DOI:10.1021/jo035557m

Reference yield:

: 81370-49-2,68198-62-9,75322-24-6,68182-93-4
cyclotriguaiacyclene

: 669692-96-0
(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / K₂CO₃ / dimethylformamide / Heating

2: 60 percent / BBr₃ / toluene / 12 h / 90 °C

With boron tribromide; potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo035557m

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 669692-96-0
(+/-)-2,7,12-trihydroxy-3,8,13-tris(4-nitrophenoxy)-10,15-dihydro-5H-tribenzo[adg]cyclononene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / K₂CO₃ / dimethylformamide / Heating

2: 60 percent / BBr₃ / toluene / 12 h / 90 °C

With boron tribromide; potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo035557m