4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

Base Information

Chemical Name:4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester
CAS No.:112799-43-6
Molecular Formula:C₁₄H₁₆O₄S
Molecular Weight:280.345
Hs Code.:

Synonyms:4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

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Chemical Property of 4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

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Technology Process of 4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

There total 4 articles about 4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 112799-47-0
Tetrahydro-2,5-dimethoxy-2-methyl-4-phenylthiofuran-3-carbonsaeuremethylester

: 112799-43-6
4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 7039-93-2
2,5-Dihydrofuran-2,5-dimethoxy-2-methylfuran-3-carbonsaeuremethylester

: 112799-43-6
4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / piperidine / propan-2-ol / 20 h / Ambient temperature

2: 75 percent / 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 12 h / Ambient temperature

With piperidine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; isopropyl alcohol;

Reference yield:

: 6141-58-8
methyl 2-methyl-3-furancarboxylate

: 112799-43-6
4,5-Dihydro-5-methoxy-2-methyl-4-phenylthio-furan-3-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Na₂CO₃, Br₂ / 3 h / -5 - 0 °C

2: 91 percent / piperidine / propan-2-ol / 20 h / Ambient temperature

3: 75 percent / 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 12 h / Ambient temperature

With piperidine; bromine; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; isopropyl alcohol;