Technology Process of C24H25NO5
There total 6 articles about C24H25NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tri-n-butyl-tin hydride;
2,2'-azobis(isobutyronitrile);
In
benzene;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) Sia2BH; 2.) 30 percent H2O2 then Jones reagent / 1.) THF, 0 deg C; 2.) 5 percent aq. NaOH, r.t.
2: ethyl acetate
3: 58 percent / butan-1-ol / 20 h / Heating
4: 58 percent / Br2 / CH2Cl2 / Ambient temperature
5: 80 percent / Bu3SnH / AIBN / benzene / Heating
With
Jones reagent; dihydrogen peroxide; bromine; tri-n-butyl-tin hydride; bis-(1,2-dimethylpropyl)borane;
2,2'-azobis(isobutyronitrile);
In
dichloromethane; ethyl acetate; butan-1-ol; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethyl acetate
2: 58 percent / butan-1-ol / 20 h / Heating
3: 58 percent / Br2 / CH2Cl2 / Ambient temperature
4: 80 percent / Bu3SnH / AIBN / benzene / Heating
With
bromine; tri-n-butyl-tin hydride;
2,2'-azobis(isobutyronitrile);
In
dichloromethane; ethyl acetate; butan-1-ol; benzene;