N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

Base Information

Chemical Name:N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine
CAS No.:1050495-20-9
Molecular Formula:C₁₈H₂₈N₆O
Molecular Weight:344.46
Hs Code.:

N<sub>2</sub>-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

Synonyms:N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

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Chemical Property of N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

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Technology Process of N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

There total 7 articles about N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1050494-43-3
2-chloro-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purin-6-amine

: 3218-02-8
cyclohexylmethylamine

: 1050495-20-9
N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

Guidance literature:: at 170 ℃; for 0.0833333h; Microwave irradiation;

Reference yield:

: 14774-37-9
(tetrahydro-2H-pyran-4-yl)methanol

: 1050495-20-9
N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 - 43 °C

2: ammonia / isopropyl alcohol / 50 °C

3: 0.08 h / 170 °C / Microwave irradiation

With di-isopropyl azodicarboxylate; ammonia; triphenylphosphine; In tetrahydrofuran; isopropyl alcohol;

Reference yield:

: 110238-91-0
tetrahydropyran-4-carboxylic acid methyl ester

: 1050495-20-9
N₂-(cyclohexylmethyl)-9-(tetrahydro-2H-pyran-4-ylmethyl)-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 10 - 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 - 43 °C

3: ammonia / isopropyl alcohol / 50 °C

4: 0.08 h / 170 °C / Microwave irradiation

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; ammonia; triphenylphosphine; In tetrahydrofuran; isopropyl alcohol;