C₂₄H₃₅IO₅Si

Base Information

Chemical Name:C₂₄H₃₅IO₅Si
CAS No.:1388153-31-8
Molecular Formula:C₂₄H₃₅IO₅Si
Molecular Weight:558.529
Hs Code.:

C<sub>24</sub>H<sub>35</sub>IO<sub>5</sub>Si

Synonyms:C₂₄H₃₅IO₅Si

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Chemical Property of C₂₄H₃₅IO₅Si

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Technology Process of C₂₄H₃₅IO₅Si

There total 19 articles about C₂₄H₃₅IO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1388152-95-1
C₂₄H₃₆O₅Si

: 1388153-31-8
C₂₄H₃₅IO₅Si

Guidance literature:: With N-iodo-succinimide; silver nitrate; In acetone; at 0 ℃; for 1h;
DOI:10.1021/ja305864z

Reference yield:

: C₂₆H₄₀O₆Si

: 1388153-31-8
C₂₄H₃₅IO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

2.2: -20 °C / Molecular sieve

3.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

5.1: N-iodo-succinimide; silver nitrate / acetone / 1 h / 0 °C

With titanium(IV) isopropylate; N-chloro-succinimide; N-iodo-succinimide; (-)-diethyl tartrate; diisobutylaluminium hydride; silver nitrate; triphenylphosphine; methyloxirane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; acetone; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388153-31-8
C₂₄H₃₅IO₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

6.2: 1 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

8.2: -20 °C / Molecular sieve

9.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

10.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -40 °C / Inert atmosphere

11.1: N-iodo-succinimide; silver nitrate / acetone / 1 h / 0 °C

With titanium(IV) isopropylate; N-chloro-succinimide; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; triethylamine; triphenylphosphine; methyloxirane; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ja305864z