C₅₁H₄₆O₂S

Base Information

Chemical Name:C₅₁H₄₆O₂S
CAS No.:775306-61-1
Molecular Formula:C₅₁H₄₆O₂S
Molecular Weight:722.991
Hs Code.:

C<sub>51</sub>H<sub>46</sub>O<sub>2</sub>S

Synonyms:C₅₁H₄₆O₂S

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Chemical Property of C₅₁H₄₆O₂S

Chemical Property:

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Technology Process of C₅₁H₄₆O₂S

There total 5 articles about C₅₁H₄₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 775306-60-0
C₆₀H₆₆O₂SSi

: 775306-61-1
C₅₁H₄₆O₂S

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ma048728d

Reference yield:

: C₂₄H₁₇Br₂O⁽¹⁺⁾*BF₄^(1-)

: 775306-61-1
C₅₁H₄₆O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: 46 percent / acetic anhydride / 2 h / 150 °C

2: 28 percent / PdCl₂(PPh₃)2; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-acetamide / 12 h / 160 °C

3: 97 percent / N-bromosuccinimide; acetic acid / CHCl₃ / Heating

4: 64 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

5: 87 percent / Bu₄NF / tetrahydrofuran / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; acetic anhydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; chloroform; N,N-dimethyl acetamide;
DOI:10.1021/ma048728d

Reference yield:

: 775306-53-1
C₂₉H₁₈S

: 775306-61-1
C₅₁H₄₆O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / N-bromosuccinimide; acetic acid / CHCl₃ / Heating

2: 64 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

3: 87 percent / Bu₄NF / tetrahydrofuran / 20 °C

With piperidine; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; chloroform;
DOI:10.1021/ma048728d