Technology Process of C31H30NOP
There total 8 articles about C31H30NOP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 9h;
DOI:10.1039/c1cc11823d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 6 h / 60 °C
3: dichloromethane / 1.5 h / 20 °C
4: sodium hydroxide / diethyl ether; water
5: triethylamine / tetrahydrofuran / 9 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; sodium hydride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1039/c1cc11823d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 6 h / 60 °C
2: dichloromethane / 1.5 h / 20 °C
3: sodium hydroxide / diethyl ether; water
4: triethylamine / tetrahydrofuran / 9 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; benzene;
DOI:10.1039/c1cc11823d
