cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

Base Information

Chemical Name:cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>
CAS No.:225116-82-5
Molecular Formula:C₄₁H₅₅Cl₂N₇O₉
Molecular Weight:860.835
Hs Code.:

Synonyms:cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

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Technology Process of cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

There total 3 articles about cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-proline TFA salt

: 225116-82-5
cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

Guidance literature:: With diphenylphosphoranyl azide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 48h;
DOI:10.1021/jm9811007

Reference yield:

: 225116-73-4
N-<(9-fluorenylmethyl)carbonyl>-asparagyl-valine

: 225116-82-5
cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

Guidance literature:: Multi-step reaction with 2 steps

2: 62 percent / 1-hydroxybenzotriazole, diphenylphosphoryl azide, diisopropylethylamine / dimethylformamide / 48 h

With diphenylphosphoranyl azide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm9811007

Reference yield:

: 2-[3-carbamoyl-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionylamino]-3-methyl-butyric acid tert-butyl ester

: 225116-82-5
cyclo-<5-amino-(pentyloxycarbonyl)-O-<(2,6-dichlorophenyl)methyl>-tyrosyl-valyl-asparagyl-valyl-prolyl>

Guidance literature:: Multi-step reaction with 3 steps

1: aq. TFA

3: 62 percent / 1-hydroxybenzotriazole, diphenylphosphoryl azide, diisopropylethylamine / dimethylformamide / 48 h

With diphenylphosphoranyl azide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm9811007