Technology Process of C29H24O3
There total 3 articles about C29H24O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide;
In
1,2-dichloro-ethane;
at 80 ℃;
for 2h;
under 760.051 Torr;
Molecular sieve;
DOI:10.1002/chem.201103924
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 2 h / -78 °C
2.1: silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide / 1,2-dichloro-ethane / 0.66 h / 80 °C / 760.05 Torr / Molecular sieve
3.1: silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide / 1,2-dichloro-ethane / 2 h / 80 °C / 760.05 Torr / Molecular sieve
With
silver hexafluoroantimonate; n-butyllithium; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide;
In
tetrahydrofuran; hexane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201103924
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide / 1,2-dichloro-ethane / 0.66 h / 80 °C / 760.05 Torr / Molecular sieve
2: silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide / 1,2-dichloro-ethane / 2 h / 80 °C / 760.05 Torr / Molecular sieve
With
silver hexafluoroantimonate; tetracarbonyldi-μ-chlorodirhodium(I); carbon monoxide;
In
1,2-dichloro-ethane;
DOI:10.1002/chem.201103924