1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene

Base Information

• Chemical Name: 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene
• CAS No.: 1284198-58-8
• Molecular Formula: C₂₄H₁₈F₆N₂OS
• Molecular Weight: 496.476

Synonyms:1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene

Chemical Property of 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene

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Technology Process of 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene

There total 2 articles about 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

3-bromo-2-methyl-5-(2-methoxylphenyl)thiophene (914360-26-2) + 2-cyano-1,5-dimethylpyrrol-4-yl-2,3,3,4,4,5,5-heptafluorocyclopentene → 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene (1284198-58-8)

Guidance literature:

3-bromo-2-methyl-5-(2-methoxylphenyl)thiophene; With n-butyllithium; In hexane; at -78 ℃; for 0.5h; Inert atmosphere;

2-cyano-1,5-dimethylpyrrol-4-yl-2,3,3,4,4,5,5-heptafluorocyclopentene; In hexane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.jphotochem.2010.07.001

Reference yield:

C24H18F6N2OS → 1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene (1284198-58-8)

Guidance literature:

In hexane; at 20 ℃; Quantum yield; Irradiation;

DOI:10.1016/j.jphotochem.2010.07.001

Reference yield:

1-(2-cyano-1,5-dimethyl-4-pyrryl)-2-[2-methyl-5-(2-methoxyphenyl)-3-thienyl]perfluorocyclopentene (1284198-58-8) → C24H18F6N2OS

Guidance literature:

In hexane; at 20 ℃; Quantum yield; UV-irradiation;

DOI:10.1016/j.jphotochem.2010.07.001

upstream raw materials:

3-bromo-2-methyl-5-(2-methoxylphenyl)thiophene

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