2,3-dimethylphenyl dimethylcarbamate

Base Information

Chemical Name:2,3-dimethylphenyl dimethylcarbamate
CAS No.:1224730-99-7
Molecular Formula:C₁₁H₁₅NO₂
Molecular Weight:193.246
Hs Code.:

Synonyms:2,3-dimethylphenyl dimethylcarbamate

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Chemical Property of 2,3-dimethylphenyl dimethylcarbamate

Chemical Property:

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Technology Process of 2,3-dimethylphenyl dimethylcarbamate

There total 1 articles about 2,3-dimethylphenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1224730-99-7
2,3-dimethylphenyl dimethylcarbamate

Guidance literature:: 2,3-Dimethylphenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; Inert atmosphere;

N,N-Dimethylcarbamoyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja100783c

Reference yield: 78.0%

: 1224730-99-7
2,3-dimethylphenyl dimethylcarbamate

: 140-88-5,9003-32-1
ethyl acrylate

: 1414838-18-8
(E)-ethyl 3-{2-[(N,N-dimethylcarbamoyl)oxy]-3,4-dimethylphenyl}acrylate

Guidance literature:: With silver hexafluoroantimonate; [RhCl₂(p-cymene)]2; copper(II) acetate monohydrate; In 1,2-dimethoxyethane; at 110 ℃; for 24h; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c2cc36196e

Reference yield: 50.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 1224730-99-7
2,3-dimethylphenyl dimethylcarbamate

: 1309752-12-2
(E)-butyl 3-(2-(dimethylcarbamoyloxy)-3,4-dimethylphenyl)acrylate

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; In TETRAHYDROPYRANE; at 110 ℃; for 24h; under 760.051 Torr; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol201140q