2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

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Chemical Name:2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol
CAS No.:778595-11-2
Molecular Formula:C₄₂H₅₃NO₇Si
Molecular Weight:711.971
Hs Code.:

2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

Synonyms:2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

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Chemical Property of 2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

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Technology Process of 2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

There total 1 articles about 2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 224578-23-8
2,2-Dimethyl-propionic acid 2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethyl ester

: 778595-11-2
2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1002/anie.200390322

Reference yield:

: 778595-11-2
2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

: 778594-95-9
(4-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[(2R,6R)-4-methylene-6-(2-triisopropylsilanyloxy-ethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-oxazol-2-yl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine

2: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂; H₂O / pH 7

With 2,6-dimethylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1002/anie.200390322

Reference yield:

: 778595-11-2
2-((2R,6R)-6-{(2R,4R,6R)-4-(tert-Butyl-diphenyl-silanyloxy)-6-[2-(4-methoxy-benzyloxymethyl)-oxazol-4-yl]-tetrahydro-pyran-2-ylmethyl}-4-methylene-tetrahydro-pyran-2-yl)-ethanol

: 553636-07-0
Methanesulfonic acid 4-{(2R,4R,6R)-4-(tert-butyl-diphenyl-silanyloxy)-6-[(2R,6R)-4-methylene-6-(2-triisopropylsilanyloxy-ethyl)-tetrahydro-pyran-2-ylmethyl]-tetrahydro-pyran-2-yl}-oxazol-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-lutidine

2: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂; H₂O / pH 7

3: triethylamine

With 2,6-dimethylpyridine; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1002/anie.200390322