1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

Base Information

Chemical Name:1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene
CAS No.:1534391-66-6
Molecular Formula:C₆₃H₁₁₀O₄
Molecular Weight:931.564
Hs Code.:

Synonyms:1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

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Chemical Property of 1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

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Technology Process of 1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

There total 4 articles about 1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1534391-75-7
diethyl [2,3-bis(dodecyloxy)benzyl]phosphonate

: 1534391-60-0
2,3-bis(dodecyloxy)-4-methylbenzaldehyde

: 1534391-66-6
1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; paraffin oil; for 6h; Inert atmosphere; Reflux;
DOI:10.5560/ZNB.2013-3170

Reference yield:

: 488-17-5
3-methylbenzene-1,2-diol

: 1534391-66-6
1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / 1,4-dioxane

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 3 h / 20 °C

2.2: 1 h / 20 °C

3.1: sodium hydride / paraffin oil; 1,2-dimethoxyethane / 6 h / Inert atmosphere; Reflux

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; potassium hydroxide; In 1,4-dioxane; 1,2-dimethoxyethane; diethyl ether; hexane; paraffin oil; 2.1: |Bouveault Aldehyde Synthesis / 3.1: |Wittig-Horner Reaction;
DOI:10.5560/ZNB.2013-3170

Reference yield:

: 1534391-57-5
1,2-bis(dodecyloxy)-3-methylbenzene

: 1534391-66-6
1-{(E)-2-[2,3-bis(dodecyloxy)phenyl]vinyl}-2,3-bis(dodecyloxy)-4-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 3 h / 20 °C

1.2: 1 h / 20 °C

2.1: sodium hydride / paraffin oil; 1,2-dimethoxyethane / 6 h / Inert atmosphere; Reflux

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; In 1,2-dimethoxyethane; diethyl ether; hexane; paraffin oil; 1.1: |Bouveault Aldehyde Synthesis / 2.1: |Wittig-Horner Reaction;
DOI:10.5560/ZNB.2013-3170