4-TERT-AMYLBENZENESULFONYL CHLORIDE

Base Information

• Chemical Name: 4-TERT-AMYLBENZENESULFONYL CHLORIDE
• CAS No.: 169677-20-7
• Molecular Formula: C11H15 Cl O2 S
• Molecular Weight: 246.758
• Hs Code.: 2904909090
• Mol file: 169677-20-7.mol

Synonyms:4-(1,1-Dimethylpropyl)benzenesulfonylchloride; 4-(1,1-Dimethylpropyl)phenylsulfonyl chloride; 4-tert-Amylbenzenesulfonylchloride; 4-tert-Pentylbenzene-1-sulfonyl chloride;4-tert-Pentylbenzenesulfonyl chloride

Chemical Property of 4-TERT-AMYLBENZENESULFONYL CHLORIDE

Chemical Property:

• Vapor Pressure: 0.001mmHg at 25°C
• Melting Point: 44-49°C
• Refractive Index: 1.519
• Boiling Point: 311.4°Cat760mmHg
• Flash Point: 142.1°C
• PSA: 42.52000
• Density: 1.179g/cm³
• LogP: 4.38250
• Sensitive.: Moisture Sensitive

Purity/Quality:

98%Min ^*data from raw suppliers

4-(tert-Pentyl)benzene-1-sulfonylchloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R34:Causes burns.
• Hazard Codes: R34:Causes burns.
• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-TERT-AMYLBENZENESULFONYL CHLORIDE

There total 2 articles about 4-TERT-AMYLBENZENESULFONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tery-amylbenzene (2049-95-8) → 4-(1,1-dimethylpropyl)benzenesulfonyl chloride (169677-20-7)

Guidance literature:

With tetrachloromethane; chlorosulphuric acid;

DOI:10.1021/ja01201a001

Reference yield:

tert-amylbenzene-4-sulphonic acid → 4-(1,1-dimethylpropyl)benzenesulfonyl chloride (169677-20-7)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; at 80 ℃; for 2h;

DOI:10.1002/ardp.201600251

Reference yield: 90.0%

4-(1,1-dimethylpropyl)benzenesulfonyl chloride (169677-20-7) + L-proline (147-85-3,25191-13-3,37159-97-0,4305-67-3,4607-28-7) → (S)-N-{p-(t-amyl)phenylsulfonyl}proline (378238-20-1)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 60 ℃;

DOI:10.1016/S0040-4020(01)00684-6

upstream raw materials:

tery-amylbenzene

Downstream raw materials:

(S)-N-{p-(t-amyl)phenylsulfonyl}proline

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