Technology Process of C27H35N3O2S
There total 8 articles about C27H35N3O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C25H33N3OS; acetic anhydride;
In
dichloromethane;
at 20 ℃;
for 3h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / dichloromethane
2: iron; acetic acid / water / 4 h / Reflux
3: sodium cyanoborohydride; acetic acid / dichloromethane
4: acetic acid / Reflux
5: tetrahydrofuran
With
pyridine; iron; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.10.091
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydroxide / ethanol / 2 h / Reflux
2: pyridine / dichloromethane
3: iron; acetic acid / water / 4 h / Reflux
4: sodium cyanoborohydride; acetic acid / dichloromethane
5: acetic acid / Reflux
6: tetrahydrofuran
With
pyridine; iron; sodium cyanoborohydride; acetic acid; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.10.091