Technology Process of tert-butyl 5-amino-2,3-dimethoxybenzylcarbamate
There total 4 articles about tert-butyl 5-amino-2,3-dimethoxybenzylcarbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; thiophene; di-isopropyl ether;
at 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / ethanol / 1 h / 50 °C
2: triethylamine / 1,4-dioxane / 20 °C
3: hydrogen / palladium on activated charcoal / tetrahydrofuran; thiophene; di-isopropyl ether / 20 h / 20 °C
With
hydrogen; hydrazine hydrate; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; thiophene; ethanol; di-isopropyl ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / 1,4-dioxane / 20 °C
2: hydrogen / palladium on activated charcoal / tetrahydrofuran; thiophene; di-isopropyl ether / 20 h / 20 °C
With
hydrogen; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; thiophene; di-isopropyl ether;
