Technology Process of 2-benzyloxy-9,10,16,17,23,24-hexa-n-butylphthalocyanine
There total 4 articles about 2-benzyloxy-9,10,16,17,23,24-hexa-n-butylphthalocyanine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C56H66N8O;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
Sonication;
benzyl chloride;
In
N,N-dimethyl-formamide;
for 1h;
DOI:10.1002/ejic.201000511
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium methanolate / i-Amyl alcohol / 3 h / Reflux
1.2: Cooling with ice
1.3: 2 h / Reflux
2.1: sulfuric acid / 0.08 h
3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Sonication
3.2: 1 h
With
sulfuric acid; lithium methanolate; sodium hydride;
In
i-Amyl alcohol; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201000511
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium methanolate / i-Amyl alcohol / 3 h / Reflux
1.2: Cooling with ice
1.3: 2 h / Reflux
2.1: sulfuric acid / 0.08 h
3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Sonication
3.2: 1 h
With
sulfuric acid; lithium methanolate; sodium hydride;
In
i-Amyl alcohol; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201000511
