(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

Base Information

Chemical Name:(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane
CAS No.:198023-08-4
Molecular Formula:C₅₁H₈₄Se₂Si₆Sn
Molecular Weight:1142.37
Hs Code.:

Synonyms:(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

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Chemical Property of (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

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Technology Process of (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

There total 2 articles about (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 198023-03-9
5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-[2,6-bis(2-isopropylphenyl)phenyl]-1,2,3,4,5-tetraselenastannolane

: 198023-08-4
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

Guidance literature:: With triphenylphosphine; In hexane; byproducts: Ph3P=Se; treatment of Sn-compd. with 2 equiv. PPh3 at room temp., Ph3P=Se filtration off, solvent removal;
DOI:10.1080/10426509708046793

Reference yield:

: 210576-57-1
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)stannylene

: 198023-08-4
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)diselenastannirane

Guidance literature:: Multi-step reaction with 2 steps

1: not given

2: triphenylphosphine / hexane

With triphenylphosphine; In hexane;
DOI:10.1021/ja972221j