(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

Base Information

Chemical Name:(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine
CAS No.:952062-42-9
Molecular Formula:C₁₉H₂₃NO
Molecular Weight:281.398
Hs Code.:

Synonyms:(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

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Chemical Property of (R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

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Technology Process of (R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

There total 3 articles about (R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-46-9
benzylamine

: 5-(benzyloxy)pent-1-en-3-yl acetate

: 952062-42-9
(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

Guidance literature:: With [(R)-(+)-5,5'-bis(diphenylphosphino)-4,4'-bi-1,3-benzodioxole][4-cyano-3-nitrobenzenecarboxylato] [1,2,3-eta-2-propenyl Ir(III)]; caesium carbonate; In tetrahydrofuran; water; at 60 ℃; for 60h; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.7b13482

Reference yield: 17.0%

: (E)-5-benzyloxy-2-pentenyl methyl carbonate

: 100-46-9
benzylamine

: 952062-42-9
(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

: (S)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

: N-(5-benzyloxy-2-pentenyl)benzylamine

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; chiral binaphthyl-based reagent; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1021/jo070998h

Reference yield:

: (E)-5-benzyloxy-2-pentenyl methyl carbonate

: 100-46-9
benzylamine

: 952062-42-9
(R)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

: (S)-N-[1-(2-benzyloxyethyl)-2-propenyl]benzylamine

Guidance literature:: With propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; chiral binaphthyl-based reagent; In tetrahydrofuran; at 20 ℃; for 10h; Title compound not separated from byproducts.;
DOI:10.1021/jo070998h