C₄₃H₃₆Cl₃OOsP₃

Base Information

Chemical Name:C₄₃H₃₆Cl₃OOsP₃
CAS No.:133361-51-0
Molecular Formula:C₄₃H₃₆Cl₃OOsP₃
Molecular Weight:958.239
Hs Code.:

C<sub>43</sub>H<sub>36</sub>Cl<sub>3</sub>OOsP<sub>3</sub>

Synonyms:C₄₃H₃₆Cl₃OOsP₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₃H₃₆Cl₃OOsP₃

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Technology Process of C₄₃H₃₆Cl₃OOsP₃

There total 1 articles about C₄₃H₃₆Cl₃OOsP₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 16971-31-6,36007-23-5
hydridocarbonylchlorotris(triphenylphosphine)osmium(II)

: 644-97-3
Dichlorophenylphosphine

: 133361-51-0
C₄₃H₃₆Cl₃OOsP₃

Guidance literature:: In benzene; heating of Os-compd. and excess PCl2Ph in benzene for 2.5 h at reflux, 10 min react. (clear soln.), further 5 min at reflux (white ppt.), cooling; addn. of n-hexane, filtration, successive washes with diethylether and n-hexane;
DOI:10.1016/0022-328X(91)86251-K

Reference yield: 100.0%

: 133361-51-0
C₄₃H₃₆Cl₃OOsP₃

: 133361-54-3,133442-85-0
OsCl₂(phenylphosphonous dichloride)(CO)(triphenylphosphine)2

Guidance literature:: With Cl₂; In tetrachloromethane; dichloromethane; byproducts: HCl; treatment of Os-complex in CH2Cl2 with excess Cl2 in CCl4, standing for 1 day (pptn.); mixture of cis/trans isomers (Cl ligands); addn. of C2H5OH, evapn. (vac.), filtration, washes with C2H5OH and n-hexane; elem. anal.;
DOI:10.1016/0022-328X(91)86251-K

Reference yield: 89.0%

: 133361-51-0
C₄₃H₃₆Cl₃OOsP₃

: 106-49-0,12221-03-3
p-toluidine

: 133361-53-2
OsHCl{phenylphosphonous chloride(p-tolylamido)}(CO)(triphenylphosphine)2

Guidance literature:: In benzene; heating of Os-complex and p-toluidine together in C6H6 for 3 h, cooling; evapn. (vac.), recrystn. from CH2Cl2/C2H5OH, filtration, washes with ethanol and n-hexane; elem. anal.;
DOI:10.1016/0022-328X(91)86251-K