2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

Base Information

• Chemical Name: 2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine
• CAS No.: 1015256-70-8
• Molecular Formula: C₄₄H₄₄N₆O₈
• Molecular Weight: 784.869

Synonyms:2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

Chemical Property of 2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

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Technology Process of 2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

There total 1 articles about 2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

(Bis(pyridin-2-ylmethyl)amino)acetic acid (113749-54-5) + 5'-O-dimethoxytrityl-2'-amino-2'-deoxyuridine (174221-86-4) → 2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine (1015256-70-8)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b712532a

Reference yield: 81.0%

2'-amino-2'-N-[N,N-bis(2-pyridylmethyl)glycyl]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine (1015256-70-8) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → 2'-amino-2'-N-(N,N-bis(2-pyridylmethyl)glycyl)-3'-O-(2-cyanoethoxy(diisopropylamino)phosphino)-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine (1015256-71-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/b712532a

upstream raw materials:

(Bis(pyridin-2-ylmethyl)amino)acetic acid

5'-O-dimethoxytrityl-2'-amino-2'-deoxyuridine

Downstream raw materials:

2'-amino-2'-N-(N,N-bis(2-pyridylmethyl)glycyl)-3'-O-(2-cyanoethoxy(diisopropylamino)phosphino)-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)uridine

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