17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

Base Information

Chemical Name:17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione
CAS No.:146443-43-8
Molecular Formula:C₄₀H₃₀N₄O₆
Molecular Weight:662.701
Hs Code.:

17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

Synonyms:17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

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Chemical Property of 17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

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Technology Process of 17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

There total 3 articles about 17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 582-17-2
2,7-Dihydroxynaphthalene

: 146443-42-7
1,3,4,6-Tetrakis(chloromethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

: 146443-43-8
17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

Guidance literature:: With tin(IV) chloride; In 1,2-dichloro-ethane; for 0.5h; Heating;
DOI:10.1021/ja00051a013

Reference yield:

: 154230-91-8
1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

: 146443-43-8
17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / SOCl₂ / CH₂Cl₂ / 16 h

2: 64 percent / SnCl₄ / 0.5 h / Heating

With thionyl chloride; tin(IV) chloride; In dichloromethane;
DOI:10.1002/recl.19931121207

Reference yield:

: 121619-22-5
1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione

: 146443-43-8
17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 4-toluenesulfonic acid / 3 h / 110 °C

2: 90 percent / SOCl₂ / CH₂Cl₂ / 16 h

3: 64 percent / SnCl₄ / 0.5 h / Heating

With thionyl chloride; toluene-4-sulfonic acid; tin(IV) chloride; In dichloromethane;
DOI:10.1002/recl.19931121207