N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

Base Information

Chemical Name:N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide
CAS No.:1403990-52-2
Molecular Formula:C₂₃H₁₈N₄O₂
Molecular Weight:382.422
Hs Code.:

Synonyms:N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

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Technology Process of N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

There total 2 articles about N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1316792-97-8
6-amino-1,3-diphenylbenzo[e][1,2,4]triazin-7-(1H)-one

: 920-46-7,26937-45-1
Methacryloyl chloride

: 1403990-52-2
N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

Guidance literature:: 6-amino-1,3-diphenylbenzo[e][1,2,4]triazin-7-(1H)-one; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h;

Methacryloyl chloride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h;
DOI:10.1021/ol302714j

Reference yield:

: 22751-79-7
1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one

: 1403990-52-2
N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)methacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-benzylhydoxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 20 - 78 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

2.2: 12 h / 20 °C

With O-benzylhydoxylamine hydrochloride; sodium hydride; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol302714j