phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

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Chemical Name:phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose
CAS No.:1346536-09-1
Molecular Formula:C₂₇H₂₄O₆S
Molecular Weight:476.55
Hs Code.:

Synonyms:phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

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Chemical Property of phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

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Technology Process of phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

There total 3 articles about phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346536-06-8
phenyl 4,6-O-benzylidene-2-O-p-toluoyl-1-thio-β-D-idopyranoside

: 1346536-09-1
phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2011.09.098

Reference yield:

: 1346536-05-7
phenyl 4,6-O-benzylidene-1-thio-β-D-idopyranoside

: 1346536-09-1
phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0.5 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

With pyridine; Dess-Martin periodane; In dichloromethane;
DOI:10.1016/j.tet.2011.09.098

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 1346536-09-1
phenyl 4,6-O-benzylidene-2-O-toluoyl-1-thio-lyxo-β-D-hexopyranosid-3-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0.5 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

With pyridine; Dess-Martin periodane; In dichloromethane;
DOI:10.1016/j.tet.2011.09.098