1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

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Chemical Name:1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate
CAS No.:1146730-35-9
Molecular Formula:C₄₃H₄₇N₃O₉
Molecular Weight:749.861
Hs Code.:

Synonyms:1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

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Chemical Property of 1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

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Technology Process of 1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

There total 1 articles about 1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1146730-27-9
1-benzyl 4-methyl 2-amino-5-(tert-butyloxycarbonylamino)terephthalate

: 139551-74-9,359766-58-8
(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-4,4-dimethylpentanoic acid

: 1146730-35-9
1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

Guidance literature:: 1-benzyl 4-methyl 2-amino-5-(tert-butyloxycarbonylamino)terephthalate; With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.0166667h;

With benzotriazol-1-ol; In dichloromethane; at 20 ℃; for 0.0166667h;

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-4,4-dimethylpentanoic acid; In dichloromethane; at 80 ℃; for 48h;
DOI:10.1002/chem.200802151

Reference yield:

: 1146730-35-9
1-benzyl 4-methyl 5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalate

: 1146730-48-4
5-(tert-butyloxycarbonylamino)-2-[(S)-4,4-dimethyl-2-(fluoren-9-ylmethyloxycarbonylamino)pentanoylamino]terephthalic acid 4-methyl ester

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 23 ℃; for 16h; under 760.051 Torr;
DOI:10.1002/chem.200802151