(S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine

Base Information

• Chemical Name: (S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine
• CAS No.: 912650-31-8
• Molecular Formula: C₂₁H₂₇NO₄S
• Molecular Weight: 389.516

Synonyms:(S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine

Chemical Property of (S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine

Chemical Property:

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Technology Process of (S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine

There total 1 articles about (S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-hydroxylamine (912650-19-2) + pivaloyl cyanide (42867-40-3) → (S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine (912650-31-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1039/b606033a

Reference yield:

(S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-O-trimethylacetylhydroxylamine (912650-31-8) → 2-benzenesulfonyl-(2R,1'S)-1-(1'-phenyl-ethyl)-aziridine (912650-26-1) + 2-benzenesulfonyl-(2S,1'S)-1-(1'-phenyl-ethyl)-aziridine (912650-27-2)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; hexane; at -40 ℃;

DOI:10.1039/b606033a

upstream raw materials:

(S)-N-(2-benzenesulfonyl-ethyl)-N-(1-phenyl-ethyl)-hydroxylamine

pivaloyl cyanide

Downstream raw materials:

2-benzenesulfonyl-(2R,1'S)-1-(1'-phenyl-ethyl)-aziridine

2-benzenesulfonyl-(2S,1'S)-1-(1'-phenyl-ethyl)-aziridine

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