benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside
CAS No.:648431-65-6
Molecular Formula:C₄₂H₄₃NO₁₁
Molecular Weight:737.804
Hs Code.:

Synonyms:benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

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Chemical Property of benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

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Technology Process of benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78246-81-8
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 260969-99-1
ethyl 2,3-di-O-benzoyl-4,6-dideoxy-1-thio-α-L-lyxo-hexopyranoside

: 648431-65-6
benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.1016/S0968-0896(03)00366-3

Reference yield:

: 648431-65-6
benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 648431-67-8
C₃₅H₃₉NO₁₁

Guidance literature:: With acetic acid; In water; at 70 ℃; for 2h;
DOI:10.1016/S0968-0896(03)00366-3

Reference yield:

: 648431-65-6
benzyl 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 2',3'-di-O-benzoyl-4',6'-dideoxy-α-L-lyxo-hexopyranosyl-(1->3)-2-acetamido-4,6-di-O-acetyl-2-deoxy-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / H₂O / 2 h / 70 °C

2: pyridine; DMAP / 20 °C

3: 63 percent / H₂; glacial acetic acid / Pd/C / 20 °C

With pyridine; dmap; hydrogen; acetic acid; palladium on activated charcoal; In water;
DOI:10.1016/S0968-0896(03)00366-3