2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

Base Information

Chemical Name:2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate
CAS No.:1581708-29-3
Molecular Formula:C₁₀H₇O₃S*C₁₈H₂₃N₂
Molecular Weight:474.624
Hs Code.:

Synonyms:2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

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Chemical Property of 2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

Chemical Property:

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Technology Process of 2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

There total 2 articles about 2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16023-36-2
2-naphthalenesulfonate

: 1519-13-7,1694-47-9,83846-70-2
2-[(E)-4-(diethylamino)styryl]-1-methyl-pyridinium iodide

: 1581708-29-3
2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

Guidance literature:: In methanol; water; acetonitrile; at 80 ℃; for 2h;
DOI:10.1016/j.saa.2014.01.064

Reference yield:

: 109-06-8
α-picoline

: 1581708-29-3
2-[2-(4-diethylaminophenyl)vinyl]-1-methyl-pyridiniumnaphthalene-2-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 4 h / Reflux

2: piperidine / methanol / 6 h / Reflux; Inert atmosphere

3: methanol; acetonitrile; water / 2 h / 80 °C

With piperidine; In methanol; water; acetone; acetonitrile;
DOI:10.1016/j.saa.2014.01.064