13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

Base Information

Chemical Name:13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III
CAS No.:204580-15-4
Molecular Formula:C₄₈H₄₈Cl₆O₁₅
Molecular Weight:1077.62
Hs Code.:

Synonyms:13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

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Chemical Property of 13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

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Technology Process of 13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

There total 2 articles about 13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 21658-35-5
3-(2-naphthyl)propionic acid

: 95603-44-4
7,10-di-(2,2,2-trichloroethyloxycarbonyl)-10-deacetylbaccatin III

: 204580-15-4
13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene; at 20 ℃; for 4h;
DOI:10.1021/jm049483y

Reference yield:

: 49711-14-0
(E)-3-(naphthalen-2-yl)acrylic acid

: 204580-15-4
13-[3-(2-naphthyl)propanoyl]-7,10-bis(2,2,2-trichloroethoxycarbonyl)baccatin III

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / RhCl(PPh₃)3

2: DCC, DMAP / CH₂Cl₂ / Ambient temperature

With dmap; hydrogen; dicyclohexyl-carbodiimide; RhCl(PPh₃)3; In dichloromethane;
DOI:10.1016/S0960-894X(97)10218-9